Details of GSAS fit for Cr2O3 674b data jun/11bmb_4716 # File no. = 4716 # No. steps = 34500 # Scan time = JUN 01, 2014 00:52 # Sample name = NIST SRM 674b (Cr2O3) # Composition = Chromium(III) oxide # Sample Comment = 0.8 mm dia Kapton # Temp (K) = 295.0 # 2theta step (deg) = 0.001 # Time per step (sec) = 0.1 # 100/Ring Current[0] = 0.984 # Monitor I0 [0] = 92666.8 # Monitor I1 [0] = 75642.1 # Gonio._radius [mm] = 1000.0 # Calibration file = 11bmb_4699_2thcorr.calib # 2Theta correction subtracted # Normalization factor = 8.3664 # Calibrated wavelength = 0.413671 GSAS Fit Summary of 11-BM Cr2O3 674b Data # by Matthew Suchomel at APS/ANL, 2014 Using GSAS/EXPGUI ************************************** lattice a = 4.95892 (refined) SRM lattice a = 4.95898 A Delta lattice a from SRM = 0.00006 A lattice c = 13.5961 (refined) SRM lattice c = 13.5959 A Delta lattice c from SRM = 0.0002 A Ce X,Y,Z = 0, 0, 0.347 (refined) Ce Uiso = 0.002 O X,Y, Z, = 0.306, 0, 0.25 (refined) O Uiso = 0.004 background = 6-term Shifted Chebyschev (type #1) GSAS Profile type 4 GU = 1.35 (refined) GV = -0.40 (refined) GW = 0.10 (refined) LX = 0.71 (refined - gives particle size of ~ 340 nm, compared with SRM cited size of 380 nm) S1 = 8.099E-02 (refined) S2 = 8.677E-04 (refined) S3 = 3.862E-03 (refined) SH/L = 0.0011 (FIXED) 2th zero (deg) = 0.00012 (refined) Absorption (mR/L) = 0.0 (FIXED) Rwp % = 9.4% chi**2 = 3.04